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An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals

Year 2021, Volume 60, Issue 3, 169 - 174, 01.09.2021
https://doi.org/10.30797/madencilik.800948

Abstract

Flotation behavior of a lead ore sample containing both sulfide and oxide Pb minerals taken from transition zone was investigated. Detailed mineralogical analyses were conducted to determine the type of lead and gangue minerals. The results revealed that galena, cerussite and pulmbogummite were the major lead minerals and observed in close association. In the flotation tests, following determination of the optimum particle size, effects of sulfidization, type of collector, and frother were examined. Potassium amyl xanthate, a modified mercaptan (Aero 412), and and the frother (Dow250) produced the best results. Use of Flash flotation was tested to reduce the flotation time and recover the fast floating liberated galena particles at coarse particle size. A locked cycle flotation test was conducted using the optimum flotation conditions to determine grade and recovery of the final concentrate that can be produced in plant scale operation.

References

  • Abkhoshk, E., Jorjani, E., Al-Harahsheh, M., Rashchi, F., & Naazari, M. 2014. Review of the Hydrometallurgical Processing of Non-Sulfide Zinc Ores. Hydrometallurgy, 153-167.
  • Bulatovic, S. 2010. Handbook of Flotation Reagent Chemistry, Theory and Practice Volume 2: Flotation of Gold, PGM and Oxide Minerals. Elsevier.
  • Drzymala, J. 2007. Mineral Processing Foundations of Theory and Practices of Minerallugy.
  • Fa, K., Miller, J., Jiang , T., & Li, G. 2005. Sulphidization Flotation for Recovery of Lead and Zinc from Oxide-Sulfide Ores. Trans. Nonferrous Met. Soc. China, 1138-1144.
  • Fuerstenau, M. C., Olivas, S. A., Herrera-Urbina, R., & Han, K. N. 1987. The surface characteristics and flotation behavior of anglesite and cerussite. International journal of mineral processing, 20(1-2), 73-85.
  • Herrera-Urbina, R., Sotillo, F., & Fuerstenau, D. 1998. Amyl Xanthate Uptake by Natural and Sulfide-Treated Cerussite and Galena. International Journal of Mineral Processing, 113-128.
  • Herrera-Urbina, R., Sotillo, F. J., & Fuerstenau, D. W. 1999. Effect of sodium sulfide additions on the pulp potential and amyl xanthate flotation of cerussite and galena. International Journal of Mineral Processing, 55(3), 157-170.
  • Liu, C., Zhang, W., Song, S., Li, H., & Jiao, X. 2019. A novel insight of the effect of sodium chloride on the sulfidization flotation of cerussite. Powder Technology, 344, 103-107.
  • Marabini, A., Ciriachi, M., Plescia, P., & Barbaro, M. 2007. Chelating Reagents for Flotation. Minerals Engineering, 1014-1025.Mining Chemicals Handbook, 2002. Cytec Industries Inc
  • Onal, G., Bulut, G., Gul, A., Kangal, O., Perek, K.T. and Arslan, F., 2005, Flotation of Aladag oxide lead–zinc ores, Minerals Engineering 18 (2005), 279–282.
  • Popov, S. R., & Vučinić, D. R. 1994. Kinetics of ethylxanthate adsorption on cerussite in alkaline media in presence or absence of dissolved lead ions. International journal of mineral processing, 41(1-2), 115-128.
  • Somasundaran, P., Lou, A. 1999. Oxide Mineral Flotation Fundementals. In B. K. Parekh, & J. D. Miller, Advances in Flotation Technology Society for Mining, Metallurgy and Exploration, Inc s. 23-43.
  • Wills, B., Napier-Munn, T. 2006. Wills' Mineral Processing Technology An Introduction to the Practical Aspects of Ore Treatment and Mineral Recovery. Elsevier Science & Technology Books.
  • Liu, R., Liu, D., Li, J., Liu, S., Liu, Z., Gao, L., ... & Ao, S. 2020. Improved understanding of the sulfidization mechanism in cerussite flotation: An XPS, ToF-SIMS and FESEM investigation. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 124508.

An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals

Year 2021, Volume 60, Issue 3, 169 - 174, 01.09.2021
https://doi.org/10.30797/madencilik.800948

Abstract

Bu çalışmada hem sülfürlü hem de oksit yapıdaki Pb minerallerini barındıran, geçiş zonuna ait bir kurşun cevherinin flotasyon davranışı incelenmiştir. Detaylı bir mineraloji analizi yapılarak kurşun ve gang mineralleri tespit edilmiştir. Kurşun minerallerinden galen ve serüzit ile birlikte plumbogummit belirlenmiş olup, oksit ve sülfürlü kurşun minerallerinin birlikte bulunduğu bir yapı görülmektedir. Flotasyon testlerinde, öncelikle tane boyutunun etkisi incelenmiş, daha sonra sülfürleştirici, toplayıcı ve köpürtücü reaktiflerin türlerinin kurşun flotasyon üzerindeki etkisi araştırılmıştır. Flotasyon testlerinde potasyum amil ksantat, modifiye merkaptan (Aero 412) ve köpürtücü (Dow250) birlikte kullanıldığı durumda en yüksek verime ulaşılmıştır. Flotasyon süresini kısaltmak ve görece iri boyutta serbestleşen kurşun tanelerinin yüzdürülmesi amacıyla flaş flotasyonun etkisi araştırılarak en uygun açık devre tasarımı yapılmıştır. En iyi flotasyon performansının elde edildiği koşularda kapalı devre flotasyon testi yapılmış ve tesis koşullarında elde edilebilecek nihai konsantre tenör ve verimleri belirlenmiştir.

References

  • Abkhoshk, E., Jorjani, E., Al-Harahsheh, M., Rashchi, F., & Naazari, M. 2014. Review of the Hydrometallurgical Processing of Non-Sulfide Zinc Ores. Hydrometallurgy, 153-167.
  • Bulatovic, S. 2010. Handbook of Flotation Reagent Chemistry, Theory and Practice Volume 2: Flotation of Gold, PGM and Oxide Minerals. Elsevier.
  • Drzymala, J. 2007. Mineral Processing Foundations of Theory and Practices of Minerallugy.
  • Fa, K., Miller, J., Jiang , T., & Li, G. 2005. Sulphidization Flotation for Recovery of Lead and Zinc from Oxide-Sulfide Ores. Trans. Nonferrous Met. Soc. China, 1138-1144.
  • Fuerstenau, M. C., Olivas, S. A., Herrera-Urbina, R., & Han, K. N. 1987. The surface characteristics and flotation behavior of anglesite and cerussite. International journal of mineral processing, 20(1-2), 73-85.
  • Herrera-Urbina, R., Sotillo, F., & Fuerstenau, D. 1998. Amyl Xanthate Uptake by Natural and Sulfide-Treated Cerussite and Galena. International Journal of Mineral Processing, 113-128.
  • Herrera-Urbina, R., Sotillo, F. J., & Fuerstenau, D. W. 1999. Effect of sodium sulfide additions on the pulp potential and amyl xanthate flotation of cerussite and galena. International Journal of Mineral Processing, 55(3), 157-170.
  • Liu, C., Zhang, W., Song, S., Li, H., & Jiao, X. 2019. A novel insight of the effect of sodium chloride on the sulfidization flotation of cerussite. Powder Technology, 344, 103-107.
  • Marabini, A., Ciriachi, M., Plescia, P., & Barbaro, M. 2007. Chelating Reagents for Flotation. Minerals Engineering, 1014-1025.Mining Chemicals Handbook, 2002. Cytec Industries Inc
  • Onal, G., Bulut, G., Gul, A., Kangal, O., Perek, K.T. and Arslan, F., 2005, Flotation of Aladag oxide lead–zinc ores, Minerals Engineering 18 (2005), 279–282.
  • Popov, S. R., & Vučinić, D. R. 1994. Kinetics of ethylxanthate adsorption on cerussite in alkaline media in presence or absence of dissolved lead ions. International journal of mineral processing, 41(1-2), 115-128.
  • Somasundaran, P., Lou, A. 1999. Oxide Mineral Flotation Fundementals. In B. K. Parekh, & J. D. Miller, Advances in Flotation Technology Society for Mining, Metallurgy and Exploration, Inc s. 23-43.
  • Wills, B., Napier-Munn, T. 2006. Wills' Mineral Processing Technology An Introduction to the Practical Aspects of Ore Treatment and Mineral Recovery. Elsevier Science & Technology Books.
  • Liu, R., Liu, D., Li, J., Liu, S., Liu, Z., Gao, L., ... & Ao, S. 2020. Improved understanding of the sulfidization mechanism in cerussite flotation: An XPS, ToF-SIMS and FESEM investigation. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 124508.

Details

Primary Language Turkish
Subjects Geosciences, Multidisciplinary
Journal Section Technical Notes
Authors

Mete Tayhan SERDENGEÇTİ> (Primary Author)
ESAN Eczacıbaşı Endüstriyel Hammaddeler San. ve Tic. A.Ş.
0000-0001-9651-2980
Türkiye


Bekir BAŞKURT This is me
ESAN Eczacıbaşı Endüstriyel Hammaddeler San. ve Tic. A.Ş.
0000-0003-1715-8667
Türkiye


Kaan ÖZÇELİK This is me
ESAN Eczacıbaşı Endüstriyel Hammaddeler San. ve Tic. A.Ş.
0000-0001-6476-5895
Türkiye


Hüseyin BAŞTÜRKCÜ This is me
ESAN Eczacıbaşı Endüstriyel Hammaddeler San. ve Tic. A.Ş.
0000-0001-7301-9317
Türkiye

Thanks Çalışmaya katkılarından dolayı Prof. Dr. Zafir Ekmekçi’ye teşekkür ederiz.
Publication Date September 1, 2021
Submission Date September 28, 2020
Acceptance Date May 1, 2021
Published in Issue Year 2021, Volume 60Issue 3

Cite

Bibtex @technical brief { madencilik800948, journal = {Scientific Mining Journal}, issn = {2564-7024}, eissn = {2587-2613}, address = {Selanik Cad. No: 19/4 06650 Kızılay-Çankaya / ANKARA - TURKEY}, publisher = {Chamber of Mining Engineers of Turkey}, year = {2021}, volume = {60}, number = {3}, pages = {169 - 174}, doi = {10.30797/madencilik.800948}, title = {An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals}, key = {cite}, author = {Serdengeçti, Mete Tayhan and Başkurt, Bekir and Özçelik, Kaan and Baştürkcü, Hüseyin} }
APA Serdengeçti, M. T. , Başkurt, B. , Özçelik, K. & Baştürkcü, H. (2021). An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals . Scientific Mining Journal , 60 (3) , 169-174 . DOI: 10.30797/madencilik.800948
MLA Serdengeçti, M. T. , Başkurt, B. , Özçelik, K. , Baştürkcü, H. "An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals" . Scientific Mining Journal 60 (2021 ): 169-174 <http://www.mining.org.tr/en/pub/issue/64904/800948>
Chicago Serdengeçti, M. T. , Başkurt, B. , Özçelik, K. , Baştürkcü, H. "An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals". Scientific Mining Journal 60 (2021 ): 169-174
RIS TY - JOUR T1 - An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals AU - Mete TayhanSerdengeçti, BekirBaşkurt, KaanÖzçelik, HüseyinBaştürkcü Y1 - 2021 PY - 2021 N1 - doi: 10.30797/madencilik.800948 DO - 10.30797/madencilik.800948 T2 - Scientific Mining Journal JF - Journal JO - JOR SP - 169 EP - 174 VL - 60 IS - 3 SN - 2564-7024-2587-2613 M3 - doi: 10.30797/madencilik.800948 UR - https://doi.org/10.30797/madencilik.800948 Y2 - 2021 ER -
EndNote %0 Scientific Mining Journal An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals %A Mete Tayhan Serdengeçti , Bekir Başkurt , Kaan Özçelik , Hüseyin Baştürkcü %T An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals %D 2021 %J Scientific Mining Journal %P 2564-7024-2587-2613 %V 60 %N 3 %R doi: 10.30797/madencilik.800948 %U 10.30797/madencilik.800948
ISNAD Serdengeçti, Mete Tayhan , Başkurt, Bekir , Özçelik, Kaan , Baştürkcü, Hüseyin . "An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals". Scientific Mining Journal 60 / 3 (September 2021): 169-174 . https://doi.org/10.30797/madencilik.800948
AMA Serdengeçti M. T. , Başkurt B. , Özçelik K. , Baştürkcü H. An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Mining. 2021; 60(3): 169-174.
Vancouver Serdengeçti M. T. , Başkurt B. , Özçelik K. , Baştürkcü H. An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Scientific Mining Journal. 2021; 60(3): 169-174.
IEEE M. T. Serdengeçti , B. Başkurt , K. Özçelik and H. Baştürkcü , "An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals", Scientific Mining Journal, vol. 60, no. 3, pp. 169-174, Sep. 2021, doi:10.30797/madencilik.800948

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